Effects of Aging Time and Sintering Temperatures on Thermal, Structural and Morphological Properties of Coralline Hydroxyapatite

Maninder Singh  Mehta; Ravinderpal  Singh

doi:10.15415/jnp.2016.32021

Authors

Maninder Singh Mehta Department of Mechanical Engineering, Sri Guru Granth Sahib World University, Fatehgarh Sahib, Punjab, India
Ravinderpal Singh Department of Mechanical Engineering, Sri Guru Granth Sahib World University, Fatehgarh Sahib, Punjab, India

DOI:

https://doi.org/10.15415/jnp.2016.32021

Keywords:

HAP, Corals, Aging Time, Sintering Temperature, BCP

Abstract

Biphasic Calcium Phosphate bioceramics belong to a group of bone substitute biomaterials comprised of an intimate mixture of Hydroxyapatite (HAP) and β-Tricalcium Phosphates. In the present work, Coralline Hydroxyapatite was synthesized using wet precipitation method. Powder particles were aged for 24 and 48 hours at 5. X-Ray Diffraction, Fourier Transform Infrared and Thermogravimetric spectroscopic techniques were used. Biphasic Calcium Phosphate was identified as the chief structural constitution of the synthetic powders. Weight fraction of Hydroxyapatite increased with the rise of sintering temperature. Aging time of 24 hours yielded maximum amount of hydroxyapatite, thus confirming optimum aging time for the synthesis of Coralline Hydroxyapatite.

Downloads

Download data is not yet available.

References

Adamopoulous, E.I, Potaridis, K, (2007). A novel computational method to quantify and analyseosteoclastic bone resorption, Journal of computational methods in science and engineering, pp. 87-91.

Ahmed, S, Ahsana, M, (2008). Synthesis of Ca-hydroxyapatite Bioceramic from Egg Shell and its Characterization,Bangladesh J. Sci. Ind. Res, 43, pp. 501-512.

Ajie, H, Kaplan, I. R, Slota, P.J, Taylor, R.E, (1990). AMS radiocarbon dating of bone osteocalcin. Nuclear Instruments and Methods, 52, pp. 433-437. http://dx.doi.org/10.1016/0168-583X(90)90452-Z

Armentano, M, Dottori, E, Fortunati, S, Mattioli, J.M, Kenny, (2010). Biodegradable polymer matrix nanocomposites for tissue engineering, Polymer degradation and stability, 95, pp. 2126-2146. http://dx.doi.org/10.1016/j.polymdegradstab.2010.06.007

Barakat, M, Khil, M. S, Sheikhd, A, Kim, H.Y, (2009). Extraction of pure natural hydroxyapatite from the bovine bones bio waste by three different methods, Journal of materials processing technology, 209, pp. 3408–3415. http://dx.doi.org/10.1016/j.jmatprotec.2008.07.040

Ben-Nissan, B, (2003). Natural Bioceramics from coral to bone and beyond, Materials Science, 7, pp. 283-288. http://dx.doi.org/10.1016/j.cossms.2003.10.001

Boutinguiza, M, Pou, J, Comesana, R, Lusquinos, F, Carlos, A.D, Leon, B, (2012). Biological hydroxyapatite obtained from fish bones, Materials science and engineering, pp. 478-486. http://dx.doi.org/10.1016/j.msec.2011.11.021

Braye, F, Irigaray, J.L, Jallot, E, Oudadesse, H, Weber, G, Deschamps, C, Deschamps, N, Frayss, P, Tourenne, P, Tixer, H, Terver, S, Lefaivre, J, Amirabadi, A, (1996). Ressorption kinetics of osseous substitute: natural coral and synthetic hydroxyapatite, Biomaterials, 17, pp. 1345-1350. http://dx.doi.org/10.1016/0142-9612(96)88682-0

Chattopadhyay, P, Pal, S, K, Singh, L and Verma, A, (2007). Synthesis of Crystalline Hydroxyapatite from Coral (Gergonaceasp) and Cytotoxicity Evaluation, Trends Biomatar. Artif. Organs, 20, pp. 142-144.

Clarke, A, Walsh, P, Maggs, C.A, (2011). Designs from the Deep Marine Organisms for Bone Tissue Engineering, Biotechnology Advances, 29, pp. 610– 617. http://dx.doi.org/10.1016/j.biotechadv.2011.04.003

Darimonta, G.L, Clootsb, R, Heinenc, E, Seideld, L, Legrand, R, (2002). In vivo behaviour of hydroxyapatite coatings on titanium implants: a quantitative study in the rabbit, Biomaterials, 23, pp. 2569–2575. http://dx.doi.org/10.1016/S0142-9612(01)00392-1

Descamps, M, Hornez, J.C, Leriche, A, (2009). Manufacture of Hydroxyapatite Beads for Medical Applications, Journal of the European Ceramic Society, 29, pp. 369–375. http://dx.doi.org/10.1016/j.jeurceramsoc.2008.06.008

Dorozhkin, S.V, (2013).A Detailed History of Calcium Orthophosphates from 1770s till 1950, Materials Science and Engineering, 33, pp. 3085–3110. http://dx.doi.org/10.1016/j.msec.2013.04.002

Dorozhkin, V.S, (2010). Calcium Orthophosphates as Bioceramics: State of the Art, Biomaterials, 1, pp. 22-107.http://dx.doi.org/10.1016/j.biomaterials.2009.11.050

Figueiredo, M, Fernando, A, Martins, G, Freitas, J, Judas, F, Figueiredo, H, (2010). Effect of the calcination temperature on the composition and microstructure of hydroxyapatite derived from human and animal bone, Ceramics International, 36, pp. 2383-2393. http://dx.doi.org/10.1016/j.ceramint.2010.07.016

Gergely, G, Weber, F, (2010). Preparation and Characterization of Hydroxyapatite from Eggshell, Ceramics International, 36, pp. 803–806. http://dx.doi.org/10.1016/j.ceramint.2009.09.020

Mehta, M.S, Singh, R.S, (2014). Effect of Aging Time and Sintering Temperatures on Structural, Morphological and Thermal Properties of Coralline Hydroxyapatite, IJRMET, 4, pp. 2249-5762

Nissan-Ben, B, Milev, A, Vago, R, (2004). Morphology of sol-gel derived nanocoated coralline hydroxyapatite, Biomaterials, 25, pp. 4971-4975. http://dx.doi.org/10.1016/j.biomaterials.2004.02.006

Oonishi, H, (1991). Orthopaedic applications of hydroxyapatite, Biomaterials, 12, pp. 171-178. http://dx.doi.org/10.1016/0142-9612(91)90196-H

Paitel, R.S, Narendra, B.D, (2009). Calcium phosphate coating for bio-implant ap plications:materials,performance factors,and methodologies,66, pp. 1-70.

Yua, S, Hariramb, K.P, Kumara, R, Cheanga, P, Aik, K.K, (2005). In vitro apatite formation and its growth kinetics on hydroxyapatite/ polyetheretherketonebiocomposites, Biomaterials, 26, pp. 2343–2352. http://dx.doi.org/10.1016/j.biomaterials.2004.07.028

Zhou, H, Lee, Jaebeom, (2011). Nanoscale hydroxyapaitepaticles for bone tissue engineering, ActaBiomateriala, 7, pp. 2769-2781.